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New-type crystalline porous materials,i.e.,porous coordination polymers(PCPs)or metal–organic frameworks(MOFs),hydrogen-bonded organic frameworks(HOFs),etc.possess modifiable and regulable structures and pores,which are potential used in wide applications,such as storage,adsorption and separation,catalysis,etc.More importantly,their high crystallinity gives a good platform to explore their structure–property relationship by using diffraction technologies.