耐环境稳定KH570改性SiO2减反膜的制备及性能研究

来源 :2016’中国溶胶-凝胶学术研讨会暨国际论坛 | 被引量 : 0次 | 上传用户:njxgfd
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
  本文采用溶胶-凝胶法,以正硅酸四乙酯为前驱体,氨水为催化剂制备标准SiO2溶胶.在溶胶老化过程中使用硅烷偶联剂KH570对溶胶改性,通过浸渍提拉法在BK7玻璃上镀膜,获得高透过率且耐环境稳定性良好的SiO2减反膜.使用原子力显微镜(AFM)、扫描电子显微镜(SEM)、UV-Vis-NIR分光光度计、傅里叶变换红外光谱仪、接触角测试仪等对薄膜的性能进行表征.结果表明:当KH570与TEOS的摩尔比为1∶2时,薄膜的透过率最高为99.46%,在90%RH湿度环境下放置两个月时间后,薄膜的透过率基本不变,表现出了良好的耐环境稳定性.
其他文献
The perfect graphene is believed to be the strongest material.However, the useful strength of large-area graphene with engineering relevance is determined by its fracture toughness, rather than the in
会议
Fiber reinforced composites (FRCs) are commonly used in the aerospace, automotive, marine, and construction industries.Interfacial adhesion is a determining parameter for the material properties and s
会议
超级隔热材料二氧化硅气凝胶被广泛用于各种航天器、飞行器的热防护中。添加遮光剂或纤维能大大改善其在高温下的隔热性能。本文中假设遮光剂颗粒为球形,掺杂纤维为无限长圆柱,通过计算遮光剂及纤维的辐射特性得到不同温度下最优掺杂粒径,并在复合材料等效热导率最小时得到不同温度下的最佳掺杂量。研究发现:遮光颗粒和纤维的最佳掺杂直径随温度增加而减小,掺杂量随温度增加而增加,研究的四种遮光剂(碳黑、SiC、ZrO2和
Graphene doped AZO thin films were prepared by sol-gel method with using metal salts and reduced grapheneoxide(rgo) as raw materials and using ethylene glycol dimethyl ether as solvent,though spin coa
Porous crack-free C/SiO2/SiC ternary composite aerogel monolith was prepared by the one-pot sol-gel method using Catechol/formaldehyde (CF) and 3-aminopropyltriethoxysilane as the organic and inorgani
Recently, more and more high power laser have been used in the vacuum environment.The effect of vacuum contamination on the thin film laser damage has gradually become the focus in high power lasers f
In this paper, the laser damage morphology and laser damage threshold of sol-gel thin films were investigated.The laser damage of sol-gel thin film was distinguished in detail.Ring damage, this type o
Graphitic carbon nitride (g-C3N4), known as an metal-free photocatalyst[1], has attracted increasing attention because of its simple preparation and stable photocatalytic activity.Besides, the utiliza
A series of different PVBCz-b-PDMAEMA star block copolymers with different arm numbers and PDMAEMA block lengths were successfully synthesized via atom transfer radical polymerization (ATRP) using the
Using commercial Lower melting point glass powers, Ce∶YAG phosphor powder and acrylic resin as raw materials, Ce∶YAG quartz glass phosphor films for high-power white LED have been successfully prepare