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The derivatives of 3,4-dialkoxythiophene have been synthesized by double Williamson etherification of the corresponding alkylhalides [3,4-dichloro-l-butene, ethyl iodoacetate, N-(2-bromoethyl)phthalimide] to yield the desired monomer.Polymerization of these derivatives or their dibromo analogs by various methods have been attempted.Characterizations of the preliminary resulting polymers are discussed.