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目的:制备瘫康Ⅰ号合剂并建立其质量标准。方法:将黄芪、当归、赤芍、川芎、桃仁、红花、地龙、石菖蒲、远志等经煎煮、过滤制成合剂。对方中黄芪进行显微鉴别;对方中黄芪、当归和川芎进行薄层色谱(TLC)鉴别;考察合剂稳定性。结果:在显微镜下,黄芪细胞清晰可见;在TLC中检出了黄芪、当归、川芎的特征斑点;合剂稳定性良好。结论:本品制备工艺可靠;所建标准可为该合剂的质量控制提供参考。
Objective: To prepare paraquat Ⅰ mixture and establish its quality standard. Methods: Astragalus, Angelica, red peony root, Chuanxiong, peach kernel, safflower, earthworm, Shichangpu, Polygalaceae and other after boiling, made of filter mixture. The other side of the Astragalus microscopic identification; each other Astragalus, Angelica and Chuanxiong thin layer chromatography (TLC) identification; study mixture stability. Results: Under the microscope, Astragalus membranaceus cells were clearly visible. The characteristic spots of Astragalus, Angelica and Chuanxiong were detected in TLC. The stability of the mixture was good. Conclusion: The preparation of this product is reliable; the established standards can provide reference for the quality control of the mixture.