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目的建立人体生物检材中的士的宁和马钱子碱的检测方法。方法用GC/NPD及GC/MS检测马钱子药渣,喝剩的马钱子药液及人体肝脏中士的宁和马钱子碱。结果建立了多种样品中士的宁和马钱子碱的定性、定量分析方法。结论本方法操作简便,定性定量准确,可靠。用此方法可以准确测定生物检材(肝脏等)的士的宁和马钱子碱含量。
Objective To establish a method for the detection of strychnine and brucine in human biological samples. Methods GC / NPD and GC / MS were used to detect the residue of Strychnos, residue of Strychnos and human strychnine and brucine. Results A qualitative and quantitative method was established for the determination of strychnine and brucine in various samples. Conclusion The method is simple, qualitative and quantitative accurate and reliable. This method allows accurate determination of strychnine and brucine in biological samples (liver, etc.).