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The compound (SiCl3)2Fe(CO)4 was synthesized and structurally characterized by X-ray single-crystal diffraction. It crystallizes in monoclinic, space group P21/n with a = 8.287(2), b = 9.829(2), c = 9.042(2), β = 96.19(3)o, V = 732.2(3)3, C4Cl6FeO4Si2,