【摘 要】
：
The title compound, C16H14N4S, has been synthesized by the reaction of pentane-2,4-dione with 5-amino-3-benzylthio-4-cyano-l-H-pyrazole in ethanol, and its crys
【机 构】
：
Institute of Elemento-Organic Chemistry
论文部分内容阅读
The title compound, C16H14N4S, has been synthesized by the reaction of pentane-2,4-dione with 5-amino-3-benzylthio-4-cyano-l-H-pyrazole in ethanol, and its crystal structure was determined by X-ray diffraction method. The crystal is of monoclinic, space group P21/n with a=8.699(3), b=23.139(9), c=7.536(3) A, β= 92.400(8)°, V= 1515.5(10) A3, Z=4,Mr=294037, Dc= 1.290 g/cm3, λ=0.71073 A,μ(MoKo)=0.212 mm-1 and F(000)=616. The structure was refined to R=0.0533 and wR=0.1141 for 2672 unique reflections with Rint= 0.06.distance of 3.875 A and the angle of 164.8°.
其他文献
Aluminum-cobalt co-substituted α-Ni(OH)2 was prepared by means of the titration method in a buffer solution, the structure was characterized by XRD analysis. W
The effect of different kinds of surfactants on the size distribution of nanodiamond particles in clean oil was studied. Results show that the dispersing stabil
IntroductionNicotinic acid and its transition-metal comple-xes have become increasingly important due to their potential applications as cosmetics or medicines
Long time behavior of solutions to semilinear parabolic equations with nonlocal nonlinear source ut - △u = ∫Ω g(u)dx inΩ× (0, T) and with nonlocal boundary
由硝酸钴水溶液和肼基甲酸甲酯(NH2NHCOOCH3, mcz)的水溶液反应, 首次制备出了配合物[Co(mcz)3](NO3)2H2O, Mr = 471.23, 测定了其晶体结构。晶体属单斜晶系, P21/n空间群。
The author presents a curvature characterization of Ricci-pseudosymmetric hypersurfaces in semi-Riemannian space forms Nns+1(c),n ≥4.
The authors consider the Cauchy problem with a kind of non-smooth initial data for quasilinear hyperbolic systems and obtain a necessary and sufficient conditio
Two new nucleoside derivatives containing benzophenoxazinone moiety were synthesized. Their luminescence spectra show that they have strong near infrared fluore
The concepts of branching chain in random environmnet and canonical branching chain in random environment axe introduced. Moreover the existence of these chains