Synthesis and Characterization of Polyamides Based on Dimer Acid

来源 :武汉理工大学学报(材料科学版)(英文版) | 被引量 : 0次 | 上传用户:titicool
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
A series of dimer acid-based polyamides were synthesized by melt-polycondensation of dimer acid and various aromatic diamines,and were characterized by Fourier transform infrared spectrum(FT-IR)and nuclear magnetic resonance(1~H NMR).The physical properties of the polyamides,such as glass transition temperature,melting temperature,decomposition temperature and mechanical properties were also investigated.The polyamides\'intrinsic viscosity ranges from 1.8 dL·g~(-1) to 2.2 dL·g~(-1),and the melting temperature ranges from 140℃to 181℃.The glass transition temperatures,observed from dynamic mechanical analysis,fall in the range of 34.8-48.2℃.The physical and mechanical properties of the resultant polyamides are similar to those of the PA1212.The heat resistance and mechanical properties of poly(4,4\'-diphenylsulfone dimeramide)(PSD)and poly(4,4\'-diphenyl dimeramide)(PPDI)are comparable to those of PA1212.
其他文献
HfTiN film was deposited by co-reactive sputtering and then was annealed in dif-ferent gas ambients at temperature of 650 ℃ for 2 min to form HfTiON film. Capacitance-voltage and gate-leakage characteristics were investigated. The N2O-annealed sample exhi