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The title compound,1-(N,N-di-(p-toluenesulfonyl))-amino-2-(N’-p-toluenesulfonyl)-amino-3,5-dinitrobenzene,was synthesized and structurally determined by single-crystal X-ray diffraction method. It crystallizes in orthorhombic,space group Pna21 with a=13.723(2),b=25.354(4),c=8.6565(12) ,V=3011.9(8) 3,Z=4,Mr=660.68,F(000)=1368,Dc=1.457 g/cm3,μ=0.309,the final R=0.0609 and wR=0.1042. The H atom of N2-H group,which is the unique recognition site to anion,is enveloped by two oxygen atoms and one benzene from two and one p-toluenesulfonyl moieties,respectively.
The title compound, 1- (N, N-di- (p-toluenesulfonyl)) -amino-2- (N’-p-toluenesulfonyl) -amino-3,5-dinitrobenzene, was synthesized and structurally determined by single-crystal X-ray diffraction method. It crystallizes in orthorhombic space group Pna21 with a = 13.723 (2), b = 25.354 (4), c = 8.6565 (12) Mr = 660.68, F (000) = 1368, Dc = 1.457 g / cm3, μ = 0.309, the final R = 0.0609 and wR = 0.1042. The H atom of N2 -H group, which is the unique recognition site to anion, is enveloped by two oxygen atoms and one benzene from two and one p-toluenesulfonyl moieties, respectively.