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A novel Schiff-base compound based on ferrocene C18H17OFeN3 (1) has been synthesized and characterized by X-ray diffraction. The title compound crystallizes in monoclinic, space group P21/c with a = 19.2343(17), b = 10.5084(9), c = 7.9373(7) , β = 97.7740°, Z = 4, V = 1589.6(2) 3, Dc = 1.451 g/cm3, μ(MoKα) = 0.956 mm-1, F(000) = 720, the final R = 0.0343 and wR = 0.0973 for 2759 observed reflections (I > 2σ(I)). Electrochemical measurements exhibit that compound 1 undergoes a reversible one-electron redox process.
A novel Schiff-base compound based on ferrocene C18H17OFeN3 (1) has been synthesized and characterized by X-ray diffraction. The title compound crystallizes in monoclinic space group P21 / c with a = 19.2343 (17), b = 10.5084 (c) = 7.9373 (7) β β = 97.7740 ° Z = 4 V = 1589.6 (2) 3 Dc = 1.451 g / cm3 μ (MoKα) = 0.956 mm -1 F , the final R = 0.0343 and wR = 0.0973 for 2759 observed reflections (I> 2σ (I)). Electrochemical measurements exhibit that compound 1 undergoes a reversible one-electron redox process.