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A nickel-1,10-phenanthroline complex supported on an octamolybdate, [{Ni(phen)2}2(x- Mo8O26)], has been hydrothermally synthesized with MoO3, H2MoO4, Ni(OAc)2· 6H2O and 1,10-phenathroline (1,10-phen) as raw materials. The crystals of the compound be