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CdS, CuxS (x=1, 2) and ZnS with different morphologies were produced by the solvothermal reactions of M(CH3COO)2·2H2O (M=Cd, Cu and Zn) and NH2CSNH2 in hexane with and without silica gel as a hard template at 200 ℃ for 24 h. The product phases were d