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A low-dimensional ion-pair compound[4-CN-Bz-4-Ph-Py][Ni(mnt)2](1,4-CN-Bz-4-Ph-Py=(4’-cyanobenzyl)-4-phenylpridinium)and mnt^2-=maleonitriledithiolate)was designed and synthesized.The cations and anions of 1 formed irregular segregated stacks along the a a