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采用透射电子显微镜(TEM)、拉曼光谱(RMS)、扫描电子显微镜(SEM)等手段,研究了C/C复合材料在刹车过程中摩擦表面层微观结构变化,建立了微结构模型;利用有限元分析方法仿真了具有微凸体的试样在摩擦过程中的温度分布。研究表明:摩擦表面除了形成一层数微米厚的摩擦层外,还在摩擦层上不均匀地覆盖一层摩擦膜;TEM及选区电子衍射图(SAED)结果显示摩擦膜大部分区域为中等织构,随着到外表面距离的减小,织构度逐渐升高,且在摩擦膜的最表面发现高石墨化度的区域;RMS同样证实摩擦表面存在局部高石墨化度区域,摩擦过程中粗糙表面微凸体的最高温度远大于摩擦平面,是导致摩擦表面应力石墨化的主要因素之一。
The microstructure of frictional surface layer of C / C composites was studied by means of transmission electron microscopy (TEM), Raman spectroscopy (RMS) and scanning electron microscopy (SEM). The microstructure model was established. The meta-analysis method simulates the temperature distribution of asperities in the friction process. The results show that in addition to forming a friction layer with a thickness of several microns, the friction surface is also covered with a non-uniform friction layer. The TEM and SAED results show that most of the friction layer is medium-sized With the decrease of the distance to the outer surface, the texture gradually increases and a region with high degree of graphitization is found on the outermost surface of the friction film. RMS also confirms the existence of a region of high degree of graphitization on the friction surface. During the rubbing process, The maximum temperature of rough surface asperities is much larger than the friction plane, which is one of the main factors that lead to the graphitization of the stress on the friction surface.