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A new mellitate complex [Cu3(μ2-mellitate)(μ2-H2O)(H2O)2·H2O]n 1 has been synthesi-zed by the reaction of mellitic acid and Cu(CH3COO)2·H2O in the presence of base. Crystallogra-phic data for 1: C12H8O16Cu3, Mr = 598.80, orthorhombic, Pbcn, a =