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以丙酮－饱和氯化钠溶液－石油醚的一步法提取分离技术制备样品溶液，采用ＧＣ－ＭＳ分析方法对人参中有机氯农药残留进行了测定。加标人参样品的测定结果表明：两个水平加标回收率：０．１０ｍｇ／ｋｇ添加水平时，除ＰＣＮＢ平均回收率为５８．３％，其它组分的平均回收率为７６．０％～９０．１％，相对标准差为９．３％～１５．０％；０．０５０ｍｇ／ｋｇ添加水平时，平均回收率为６２．３％～８７．２％，相对标准差为６．０％～２２．５％。应用本方法测定人参中有机氯农药残留，基本上满足了灵敏、快速、准确可靠的分析方法要求
The sample solution was prepared by one-step acetone-saturated sodium chloride solution-petroleum ether extraction and separation, and the residues of organochlorine pesticides in ginseng were determined by GC-MS. The results of spiked samples showed that the recoveries of two spiked spiked samples at the level of 0.10mg / kg were 58.3% except for PCNB and 76.0% 90.1%, and the relative standard deviation was 9.3% ~ 15.0%. The average recovery was 62.3% ~ 87.2% at the level of 0.050mg / kg, the relative standard deviation was 6.0% ~ 22.5%. The determination of organochlorine pesticide residues in ginseng by this method basically meets the requirements of sensitive, rapid, accurate and reliable analytical methods