论文部分内容阅读
目的:建立痔特佳片中组成成分的鉴别与含量测定方法。方法:采用薄层色谱法对该制剂中的槐角、枳壳和当归进行了鉴别;采用高效液相色谱法测定槐角中芦丁的含量。结果:薄层鉴别斑点清晰,重复性好;含量测定平均回收率为100.14%,RSD为0.78%,方法可行。结论:所建立的方法可对痔特佳片进行有效的质量控制。
OBJECTIVE: To establish the identification and content determination method of the components in Qidiaojia Tablets. METHODS: Tilletella striata, Citrus aurantium and Angelica sinensis were identified by TLC. HPLC was used to determine the rutin content in the horns. Results: The discriminating spots were clear and the repeatability was good. The average recovery of the assay was 100.14% and the RSD was 0.78%. The method was feasible. Conclusion: The established method can effectively control the quality of the special tablets.