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在石油地球化学研究中,对有机氧一般采用国外进口的元素分析仪进行测定。由于条件的限制,我们引用大连第二仪表厂出品的SOM-1型脉冲加热-气相色谱仪,对有机氧测定的各种条件进行了试验。试验证明,操作简便、性能稳定、方法可靠。 1.仪器、试剂及操作 SOM-1型脉冲加热-气相色谱仪; 氩气(99.99%)、分子筛(5埃、40—60目)、石墨坩埚(采用光谱纯石墨电极车制而成);
In the research of petroleum geochemistry, the organic oxygen is usually measured by the elemental analyzer imported from abroad. Due to the limitations of the conditions, we quoted the SOM-1 pulse heating-gas chromatograph manufactured by Dalian No.2 Dashidian Factory and tested the conditions for the determination of organic oxygen. Test proved that easy to operate, stable performance, reliable method. 1. Instruments, reagents and operation SOM-1 pulse heating - gas chromatograph; argon gas (99.99%), molecular sieve (5 angstroms, 40-60 mesh), graphite crucible