目的:建立萨热十三味鹏鸟丸的质量标准。方法:用薄层色谱法对木香、藏菖蒲、沉香、甘草、麝香进行定性鉴别;用高效液相色谱法对诃子中没食子酸进行含量测定。结果:没食子酸在0.242 5～3.637 5μg呈良好的线性关系(r=0.999 7),平均加样回收率为99.31%,RSD 1.80%(n=9)。结论:方法专属性好,灵敏度高,可用于萨热十三味鹏鸟丸的质量控制。 OBJECTIVE: To establish the quality standard of Sagittarius Peng Peng Nong Pills. Methods: The qualitative identification of woody, calamus, incense, licorice and musk by TLC, and the determination of gallic acid in myrobalan by high performance liquid chromatography. Results: The linearity of gallic acid was 0.242 5 ~ 3.637 5μg (r = 0.999 7). The average recovery was 99.31% and the RSD was 1.80% (n = 9). Conclusion: The method is of good specificity and high sensitivity, which can be used for the quality control of Saguetongpeng Pengniao Pills.