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定量给出了液滴法制备玻璃微球壳（ Ｈ Ｇ Ｍ ）的直径与壁厚之间的依存关系，确定了制备大直径薄壁 Ｈ Ｇ Ｍ 的液滴炉温度分布、抽气速率、溶液浓度和液滴发生器操作参数等工艺条件，制备出直径为３００～４５０μｍ 、壁厚为０．７～１．２μｍ 、尺度比为３００～７００ 的 Ｈ Ｇ Ｍ ，表面粗糙度优于 １０ｎｍ ，球形度和同心度均优于 ９７％ ，耐外压能力大于 ０．９１ Ｍ Ｐａ，耐内压能力至少大于 ０．４３ Ｍ Ｐａ。
The dependence of the diameter and the wall thickness of the glass microsphere shell (HGM) prepared by the drop method was quantitatively determined. The temperature distribution, the pumping rate and the solution velocity of the droplet furnace for the preparation of the large diameter thin wall HGM were determined. Concentration and droplet generator operating parameters of the process conditions to prepare a diameter of 300 ~ 450μm, a wall thickness of 0.7 ~ 1.2μm, the scale ratio of 300 ~ 700 HG M, surface roughness better than 10nm, spherical Degree and concentricity are better than 97%, resistance to external pressure greater than 0.91 M Pa, resistance to internal pressure of at least greater than 0.43 M Pa.