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A novel coordinated polymer [(C22H50N2)(Ag2I4)]n([C22H50N2]^2+= N,N′-1,2-ethylence-bis(N,N′-dimethyl octane ammonium) (EDO)) was synthesized by the reaction of AgI and EDO at room temperature with pH = 6.8, and structurally characterized by means of X-ray