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Vilsmeier-Hasek反应的改进[BlaserDetal.OrgPrepProcedInt,1993;25:338]等摩尔的草酰氯在40~50℃加入N-甲基-N-甲酰苯胺中,然后室温搅拌12h,经后处理、蒸馏得对-(N-甲基氨基)苯甲醛,收率...
Improvement of Vilsmeier-Hasek reaction [BlaserDetal. OrgPrep ProcedInt, 1993; 25: 338] Equimolar oxalyl chloride was added to N-methylformamidilide at 40-50 ° C and then stirred at room temperature for 12 h. After workup, ) Benzaldehyde, yield ...