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A series of rare earth complexes Tb1-xEux(MAA)3phen (x=0.00,0.01,0,03,0.05,0.07,0.09,0.10,0.30,and 0.50) were synthesized with MAA as the first ligand and phen as the second ligand.The complexes were characterized by means of FT-IR,thermogravimetry-differ