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A hydrogen-bonded three-dimensional cobalt(Ⅱ) compound, {[Co(2,2′-bipy)-(Hbtc)(HaO)3].3HaO}n 1 (H3btc =1,3,5-benzenetricarboxylic acid, 2,2′-bipy = 2,2′-bipyridine), has been synthesized and characterized by single-crystal X-ray diffraction analysis, IR a