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目的:对金玄痔科熏洗散及有效部位新制剂进行GC-MS分析,建立了有效部位新制剂的GC-MS指纹图谱。方法:采用GC-MS方法对金玄痔科熏洗散及有效部位新制剂中的主要组分进行分析,并确定指纹图谱中的特征指纹信息。结果:对10个批次的有效部位新制剂进行了测定,并得到了较为理想的包含特征信息的有效部位新制剂的GC-MS指纹图谱。结论:方法重复性好,所建立的指纹图谱为金玄痔科熏洗散有效部位新制剂的质量控制提供了有效手段。
OBJECTIVE: To establish a GC-MS fingerprint of the new preparation of effective part by GC-MS. Methods: GC-MS method was used to analyze the main components of Jinxuan Hemorrhoid Washing Powder and the new preparation of effective part, and to identify the fingerprint information of the fingerprint. Results: The new formulations of the active fractions of 10 batches were determined and the GC-MS fingerprints of the new formulations of the effective fractions containing the characteristic information were obtained. Conclusion: The repeatability of the method is good. The established fingerprint provides an effective method for quality control of the new preparation of effective part of Jinxuan Hemorrhoid Washing Powder.