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The title complexes [Co^Ⅲ(TPA)(N3)2].(C104) 1 and [Cu^Ⅱ(TPA)(N3)].(C104) 2have been synthesized and characterized by single-crystal X-ray diffraction. The crystal of 1 is ofmonoclinic, space group P2t/n with a = 10.734(3), b = 13.112(4), c = 15.327(4)