微波作用下1,5-苯并硫氮杂(艹卓)-α-溴代-β-内酰胺衍生物的合成

来源 :有机化学 | 被引量 : 0次 | 上传用户:jackzhao1
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
1,5-苯并硫氮杂(艹卓)、溴乙酰氯在三乙胺的存在下,用微波辐射合成了5个新的1,5-苯并硫氮杂(艹卓)-α-溴代-β-内酰胺衍生物,并且还合成了已用常规方法合成出的9个1,5-苯并硫氮杂(艹卓)-β-内酰胺衍生物,对其结构进行了表征.文中研究了微波促进这类反应的最佳反应条件.
其他文献
AIM: To evaluate the safety of donors in adult living donor liver transplantation (LDLT) using the right lobe in a single liver transplantation center in China.
AIM: To investigate the role of endogenous pain modulatory mechanisms in the central sensitization implicated by the visceral hypersensitivity demonstrated in p
Hypersensitivity reactions (HSR) to oxaliplatin in patients with colorectal cancer include facial flushing, erythema,pruritis, fever, tachycardia, dyspnea, tong
AIM: To examine the anti-ulcerogenic and antioxidant effects of aqueous extracts of Foeniculum vulgare (FVE) on ethanol-induced gastric lesions in rats.METHODS:
An extremely rare case of persistent omphalomesenteric duct causing small bowel obstruction is presented. A 20-year-old female patient without medical history p
Background The recent studies have shown that visual performance might be affected by the ocular aberration after the corneal refractive surgery, and try to min
AIM: To establish the role of human T Cell Factor-4 (hTCF-4) gene exons 3-9 mutation status in association with sporadic rectal cancer with microsatellite insta
AIM: To investigate H+, K+-ATPase inhibition,anti-H pylori, antioxidant, and the in vivo antiulcer potential of a pectic polysaccharide from Swallow root (Decal
研究了一种包含西佛氏碱和萘酰亚胺新型材料的LB膜的制备,并采用二次谐波产生的方法研究了LB单层膜的二阶非线性光特性.这种化合物具有较大的二阶非线性极化率(χ(2)=1.51×1