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合成并制备了直键淀粉-三(苯基氨基甲酸酯)涂敷型手性固定相,利用高效波相色谱法首次直接拆分了4种外消旋硫代缩水甘油醚,并考察了流动相中异丙醇体积分数对拆分及保留的影响。
Synthesis and preparation of direct bond starch - tris (phenyl carbamate) coated chiral stationary phase, the first direct resolution of four kinds of racemic thioglycidyl ether using high performance liquid chromatography, and investigated Effect of isopropanol volume fraction on resolution and retention in mobile phase.