【摘 要】
:
研究以钛酸丁酯和氯化锶为原料,采用溶胶-沉淀法合成纳米钛酸锶(SrTiO3),通过对产物X射线衍射分析,可知NaOH浓度对产物结构具有较大影响;研究不同淀粉添加量与纳米SrTiO3粒度
【机 构】
:
沈阳理工大学材料学院非金属材料研究所,
论文部分内容阅读
研究以钛酸丁酯和氯化锶为原料,采用溶胶-沉淀法合成纳米钛酸锶(SrTiO3),通过对产物X射线衍射分析,可知NaOH浓度对产物结构具有较大影响;研究不同淀粉添加量与纳米SrTiO3粒度分布之规律,通过改变淀粉配量可有效地控制纳米SrTiO3粒度分布;通过透射电子显微镜和扫描电子显微镜对产品形态和结构进行表征,所得纳米SrTiO3形态比较规则,多数呈球形颗粒,单分散性好,粒径分布为30~80nm。讨论溶胶-沉淀法制备纳米SrTiO3的反应过程,阐明淀粉对纳米SrTiO3粒度调控作用。
In this paper, strontium titanate (SrTiO3) was synthesized by sol-precipitation method using butyl titanate and strontium chloride as raw materials. The XRD results showed that the concentration of NaOH had a significant effect on the product structure. The particle size distribution of nano SrTiO3 and the rules of nano-SrTiO3 particle size distribution can be effectively controlled by changing the particle size distribution of SrTiO3 nano-SrTiO3 by transmission electron microscopy and scanning electron microscopy morphological and structural characterization of the resulting nano-SrTiO3 morphology rules, the majority of spherical particles , Monodispersity, particle size distribution of 30 ~ 80nm. The reaction process of preparing SrTiO3 nanocomposite by sol-precipitation method was discussed, and the effect of starch on the particle size regulation of nanoscale SrTiO3 was clarified.
其他文献
通过对网络环境下读者、出版社新的特点分析,结合本馆开展的创新实践,力求探寻一条在网络条件下图书采访的新模式。
Through the analysis of the new features of readers
双宾语结构是现代汉语语法研究的一个重点,一般认为它的语序是(S)+V+O间+O直,但在光山方言中双宾结构还有另一种语序,即(S)+V+O直+O间。为了述说方便把前者称句式Ⅰ,后者称句
This paper studies the long time behavior of solutions to the Navier-Stokes equations with linear damping on R2.The authors prove the existence of L2-global att
在大气和大气与SO2气体混合污染条件下研究了NaCl对Mg-Al-Ca合金腐蚀情况的影响,讨论了镁合金腐蚀动力学、腐蚀产物及微观组织腐蚀形貌的变化情况。NaCl在大气中生成的腐蚀产
In this paper we discuss the bounds for the modulus of continuity of the blow-up time with respect to three parameters of λ, h, and p respectively for the init
本文以一次优质课观摩活动为基础,通过分析和反思课堂教学中的缺陷和不足,试图寻找解决问题的对策。
In this paper, based on a high quality class observation activitie
Objective To observe the surface structures of cardiovascular endothelial cells in situ with atomic force microscope (AFM). Methods Fresh aorta and aortic valve
目的 研究百草枯(PQ)对肝脏的损伤作用及其机制,并用抗氧化药物N-乙酰半胱氨酸(NAC)和谷胱甘肽(GSH)干预,观察药物对PQ中毒大鼠的肝脏保护作用并探讨药物作用机制.方法 33只
采用二元单体胶束共聚,合成了孪尾疏水改性丙烯酰胺/N,N-二辛基丙烯酰胺二元共聚物[简称P(AM/DiC8AM)],成功引入了疏水单体。用FTIR分析了各基团峰的归属,证明了共聚物为带有
In this paper,we give a necessary and sufficient condition for the existence of P3-factors in the line graph of a tree.Then we present an algorithm to determine