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在水热条件下,使用邻苯二胺和草酸合成了一种新的化合物邻苯二草酰胺.通过X-射线单晶衍射技术确定该化合物的结构,该化合物属于三斜晶系,P-1空间群.该化合物结构最显著的特点是存在着具有四水的水簇结构,氢键和π-π作用将该化合物连接成三维的超分子网络结构.用元素分析、红外光谱、紫外光谱对该化合物进行了表征,并测定了其荧光性能.
A new compound, phthalamide, was synthesized using o-phenylenediamine and oxalic acid under hydrothermal conditions.The structure of the compound was confirmed by X-ray single crystal diffraction and belongs to triclinic system, P- 1 space group.The most prominent feature of the structure of this compound is the existence of a water cluster structure with a four-water structure, which is connected by a hydrogen bond and a π-π interaction to form a three-dimensional supramolecular network structure.Using elemental analysis, infrared spectroscopy, The compound was characterized and its fluorescence was measured.