以十八烷醇和二乙醇胺为起始原料,设计两条路线,通过甲磺酸酯化和N-烷基化等几步反应高收率的合成出抗静电剂1800,对得到的产品进行红外、质谱和核磁的测试,并对反应影响因素进行深入的研究及优化实验条件。反应条件温和,总收率88%。 Starting from stearyl alcohol and diethanolamine, two routes were designed and the antistatic agent 1800 was synthesized in high yield by a few steps of mesylate and N-alkylation reactions. The obtained product was subjected to infrared , Mass spectrometry and nuclear magnetic test, and the factors affecting the reaction in-depth study and optimization of experimental conditions. The reaction conditions are mild, the total yield of 88%.