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在先前的文献中描述了一种空气冷却的测试管,该测试管拥有一系列的插座和插头(在结晶过程中使用的转换插座),可以安装在实验室箱式熔炉中。该装置的用途是调节物质在坩埚槽中结晶过程的晶面和结晶速率。在本文中我们讨论一种改进型的内部冷却器——锯齿状的空气冷却管(结晶架)。这种改进型的冷却器可以简单地搭建和操作,可以延长和弯曲成为各种形状,可以用于坩埚和熔炉管中。该冷却器可以通过简单的调控对不同结晶参数和物质同步进行结晶测试,利用实验用熔炉就可以达到从一系列新型的具有层状晶体结构的化合物中得到晶体的目的。
In the previous literature, an air cooled test tube was described that has a series of sockets and plugs (conversion sockets used during the crystallization process) that can be installed in a laboratory box furnace. The purpose of the device is to adjust the crystal plane and crystallization rate of the substance during the crystallization in the crucible tank. In this article we discuss an improved internal cooler - serrated air cooling tube (crystallizer). This improved cooler can be simply constructed and operated, lengthened and bent into a variety of shapes for use in crucibles and furnace tubes. The cooler can be crystallized and tested synchronously with different crystallization parameters and substances by simple regulation. The purpose of obtaining crystals from a series of novel compounds with layered crystal structure can be achieved by the experimental furnace.