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The crystal of the title compound Sr6Gd0.61Sc1.39(BO3)6 (Mr = 1037.00) was grown by Czochralski method. It crystallizes in trigonal, space group 3Rwith a = 12.415(2), c = 9.274(2) ? Z = 3, V = 1238.0(4) 3, Dc = 4.173 g/cm3, l(MoKa) = 0.71073 ? m = 22.278 mm-1, F(000) = 1411, S = 1.213, the final R = 0.0577 and wR = 0.1414 for 401 observed reflections with I>2s(I). In the structure Gd(1)O6 (Gd(1) = Gd0.46 + Sc0.54) and Gd(2)O6 (Gd(2)= Gd0.15 + Sc0.85) are alternately stacked between the planar triangular BO3 groups to form chains extending along the trigonal axis. These chains are connected through the 9-coordinate Sr atoms.
It crystallizes in trigonal, space group 3Rwith a = 12.415 (2), c = 9.274 (2). Z = The final R = 0.0577 and wR = 3, V = 1238.0 (4) 3, Dc = 4.173 g / cm3, l (MoKa) = 0.71073? M = 22.278 mm-1, In the structure Gd (1) O6 (Gd (1) = Gd0.46 + Sc0.54) and Gd (2) O6 (Gd (2) = Gd0.15 + Sc0.85) are alternately stacked between the planar triangular BO3 groups to form extending along the trigonal axis. These chains are connected through the 9-coordinate Sr atoms.