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本文提出了一个氢化物发生一冷原子荧光法间接测定痕量锑的新方法。考察了各种实验条件,并将此法用于水及沉积物标样分析,结果令人满意,对水中锑检出限为0.1μg/L,回收率96％～102％。
In this paper, a new indirect method for the determination of trace antimony by hydride generation of cold atomic fluorescence spectrometry was proposed. Various experimental conditions were investigated, and the method was applied to the standard analysis of water and sediment samples. The results were satisfactory. The detection limit of antimony in water was 0.1μg / L with the recovery of 96% -102%.