Preparation and Properties of Macroporous Silicon Nitride Ceramics by Gelcasting and Carbonthermal R

来源 :材料科学技术学报(英文版) | 被引量 : 0次 | 上传用户:wuxirl
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
Macroporous silicon nitride (Si3N4) ceramics with high strength, uniform structure and relatively high porosity were obtained by gelcasting and carbonthermal reaction in a two-step sintering technique. Microstructure and composition were investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction(XRD). Open porosity, pore size distribution and basic mechanical performance were measured by Archimedes method,mercury intrusion porosimetry and three-point bending methods, respectively. SEM and TEM results revealed that pores were formed by elongated β-Si3N4. SADP measurement proved the formation of SiC particles. The SiC granules were beneficial for the formation of high ratio elongated β-Si3N4, and at proper amount, they also acted as reinforcement phase. Thermodynamic analysis indicated that the mechanisms of the reactions were mainly associated with liquid-solid reaction and gas-liquid reaction.
其他文献
This paper proposed a multi-agent based architecture for outdoor mobile robot navigation where event-driven control is used to handle the dynamically changing o
Titanium diboride based composites, good candidates for contact materials, have high hardness, Youngs modulus,high temperature stability, and excellent electric
Selective laser sintering (SLS) is a new process to prepare the polystyrene (PS)/Al2O3 nanocomposites. In this paper, with different laser power and other proce
Several important properties of the micron-powdered Sn-Ag-Cu-Ce solder, including the spreadability, spreading ratio, wetting time, and melting point, were inve
TiO2/(O + β)-Sialon multiphase ceramics were prepared with nano Ti O2 (anatase) powder and (O + β)-Sialon powder as raw materials. Effect of Yb2O3 additive on
Software architectures shift the focus of developers from lines-of-code to coarser-grained architectural elements and their overall interconnection structure. T
Micro-laminated ZrO2-Al2O3 coatings were prepared by electrochemical depositing ZrO2 film and Al2O3 film alternatively in ethanol solutions containing aluminum
Fuel cell using borohydride as the fuel has received much attention. AB5-type hydrogen storage alloy used as the anodic material instead of noble metals has bee
The formation, thermal stability and mechanical properties of Misch metal (Mm)-based alloy bulk metallic glasses (BMGs) with composition of Mm55Al25Cu10Ni5Co5 w
White body-color (Y, Gd)BxV1- xO4-x :Eu3 + phosphors were prepared by coprecipitation reaction. Under VUV excitation at 147 nm, the red emission colorimetric pu