【摘 要】
：
Six novel thiosemicarbazones containing sugar and thiosemicarbazide moieties were synthesized by a five-step procedure using D-galactose and D-xylose as the sta
【机 构】
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College of Chemistry and Molecular Engineering
【基金项目】
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国家自然科学基金;教育部新世纪优秀人才支持计划;The Start-up Fund for Doctoral Scientific Research of Qingdao University of Science and Technology
论文部分内容阅读
Six novel thiosemicarbazones containing sugar and thiosemicarbazide moieties were synthesized by a five-step procedure using D-galactose and D-xylose as the starting materials and the corresponding glycosyl isothiocyanates as the intermediates. The target compounds were characterized by IR, 1H NMR, and elemental analysis. The coupling constants between H1 and H2 in the sugar rings, all fall within the range of J=9.2-10.0 Hz, confirming the β-configuration of the compounds.
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