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A simple one step,reproducible,synthesis route for carbon nanotubes was proposed.No external catalyst was used for the synthesis.These nanotubes were obtained after decomposition of acetone at 650 ℃ in a specially designed autoclave.The pressure generated due to decomposition of acetone played a vital role in the synthesis.The X-ray diffraction pattern and transmission electron microscopy of the sample showed that the diameter of nanotubes is in the range of 3—14 nm.The thermo gravimetric analysis showed 3%weight loss below500 ℃;the content of amorphous carbon is very less.The growth mechanism of CNTs was also proposed in the present paper.
A simple one step, reproducible, synthesis route for carbon nanotubes was proposed. No external catalyst was used for the synthesis. These nanotubes were obtained after decomposition of acetone at 650 ° C in a specially designed autoclave. a vital role in the synthesis. The X-ray diffraction pattern and transmission electron microscopy of the sample showed that the diameter of nanotubes is in the range of 3-14 nm. The thermo gravimetric analysis showed 3% weight loss below 500 ° C .; the content of amorphous carbon is very less. The growth mechanism of CNTs was also proposed in the present paper.