在直径149 mm液体喷射环流反应器(LJLR)中对三氯氧磷合成的氧化过程进行了研究,与釜式反应器相比反应时间由40 h缩短至8 h,氧气消耗量为理论量并且无尾气排放,研究结果已经用于工业生产。 Oxidation of phosphorus oxychloride in a 149 mm diameter liquid jet loop reactor (LJLR) was studied. The reaction time was shortened from 40 h to 8 h compared to the kettle reactor. The oxygen consumption was the theoretical amount and No exhaust emissions, the findings have been used for industrial production.