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The thermal decomposition reaction of the ［Zn(NFA)2(NO3)2］*2H2O(NFA=C16H18FN3O3,norfloxacin) was studied in a static atmosphere using TG-DTG and DTA methods. The thermal decomposition processes of the complex were determined and its kinetics was investigated. The kinetic parameters were obtained from analysis of the TG-DTG curves by differential and integral methods. The most pro-bable mechanism for the second stage was suggested by comparision of the kinetic parameters.