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运用高压静电纺丝和程序升温焙烧的方法制备了α2-K8P2W17MnO61纳米纤维。通过红外光谱(FT-IR)和X射线粉末衍射(XRD)对纤维进行了表征.结果表明,制备的纳米纤维为纯杂多酸盐α2-K8P2W17MnO61,扫描电子显微镜(SEM)图形显示焙烧后获得纳米纤维的平均直径大约为140 nm.
Α2-K8P2W17MnO61 nanofibers were prepared by high-pressure electrospinning and temperature programmed roasting. Fibers were characterized by infrared spectroscopy (FT-IR) and X-ray powder diffraction (XRD). The results showed that the prepared nanofibers were pure heteropolyacid salts α2-K8P2W17MnO61. The scanning electron microscopy (SEM) images showed that the average diameter of nanofibers obtained after calcination was about 140 nm.