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目的建立胆舒胶囊和胆舒软胶囊的GC指纹图谱。方法采用弹性石英毛细管色谱柱HP-Innowax(30 m×320μm,0.25μm),程序升温。结果分析了13批样品,确立了15个共有峰,建立了相似度较高(均>0.97)的胆舒胶囊和胆舒软胶囊的GC指纹图谱。结论所用方法简便、精密度高、稳定性和重复性好,可作为胆舒胶囊和胆舒软胶囊质量的控制方法。
Objective To establish the GC fingerprints of biliary capsule and biliary soft capsule. Methods Flexible quartz capillary column HP-Innowax (30 m × 320 μm, 0.25 μm) was used to program the temperature. Results Thirteen batches of samples were analyzed and 15 common peaks were established. The GC fingerprints of Ganshu Capsule and Ganshu Soft Capsule were established with high similarity (> 0.97). Conclusion The method is simple, high precision, good stability and reproducibility, and can be used as a control method for the quality of biliary capsule and biliary soft capsule.