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Dibenzyltin bis(dithiotetrahydropyrrolocarbamate) was synthesized by the rea ction of dibenzyltin dichloride with dithiotetrahydropyrrolocarbamate. The compo und was characterized by elemental analysis, IR, 1H NMR and MS. and the crystal structure was determined by X-ray single crystal diffraction. The crystal bel ongs to orthorhombic with space group Pccn, a=2.1665(6)nm, b=0.9932(3)nm, c=1.19 79(3)nm,á=90a=90?=90穋m-3,ì (MoKá)=1.330mm-1,F(000)=1208,R1=0.0341, wR2=0.0627. In the crystals, the str uctures consist of discrete molecules in which the tin atom is six-coordinate in a distorted octahedron configuration. CCDC: 179919.
Dibenzyltin bis (dithiotetrahydropyrrolocarbamate) was synthesized by the reation of dibenzyltin dichloride with dithiotetrahydropyrrolocarbamate. The compo und was characterized by elemental analysis, IR, 1H NMR and MS. And the crystal structure was determined by X-ray single crystal diffraction. The crystal bel (MoKa) ongs to orthorhombic with space group Pccn, a = 2.1665 (6) nm, b = 0.9932 (3) nm, c = 1.1979 (3) nm, = 1.330 mm-1, F (000) = 1208, R1 = 0.0341, wR2 = 0.0627. The crystals, the str uctuations consist of discrete molecules in which the tin atom is six-coordinate in a distorted octahedron configuration. CCDC: 179919 .