论文部分内容阅读
以2-氯-6-三氯甲吡啶为原料,利用三氟化锑反应合成标题化合物。通过MS和NMR分析对产物的结构进行了表征。该合成路线的优点是反应条件温和、无溶剂、收率较高。
The title compound was synthesized from 2-chloro-6-trichloropyridine using antimony trifluoride as a starting material. The structure of the product was characterized by MS and NMR analysis. The advantages of this synthetic route are mild reaction conditions, no solvent, high yield.