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介绍以高效液相色谱法测定 N,N’-双(仲丁基)-对-苯二胺(DBPD)含量.方法使用 spherisorb- NH_2柱,甲醇:三氯甲烷=60:40(V/V)为流动相,263nm处检测.方法简单,快速,回收率为95.6%~ 105%,变异系数不大于2.1%.
The content of N, N’-bis (sec-butyl) -p-phenylenediamine (DBPD) was determined by high performance liquid chromatography. Methods Spherisorb-NH_2 column was used with methanol: chloroform = 60:40 (V / V) as mobile phase and detected at 263nm. The method is simple and rapid, the recovery rate is 95.6% ~ 105%, the coefficient of variation is not more than 2.1%.