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本文叙述AHG-1型半自动氢化物装置的结构和性能的试验结果,该装置主要由氢化物反应瓶,加硼氢化钾还原剂的蠕动泵(自制)和电热石英管原子化器和载气、封气系统所组成。装置配有三个电磁阀,用程序控制器进行顺序操作。往反应瓶中加入酸性分析溶液后,只需要拔下“发生”按扭即能自动进行分析。装置主要技术数据:蠕动泵输液量～25毫升/分;反应瓶体积100或120毫升。石英管总长170毫米,有效长150毫升,内径8毫米。石英管外绕0.4毫
This article describes the experimental results of the structure and performance of the AHG-1 semi-automatic hydride device. The device mainly consists of a hydride reaction bottle, a peristaltic pump (self-made) with a potassium borohydride reducing agent and an electric quartz tube atomizer and a carrier gas, Gas seal system is composed. The unit is equipped with three solenoid valves, which are sequenced with the program controller. After adding the acidic analysis solution to the reaction flask, just unplug the “occurred” button to automatically analyze. Device main technical data: peristaltic pump infusion ~ 25 ml / min; reaction bottle volume 100 or 120 ml. Quartz tube length 170 mm, effective length 150 ml, diameter 8 mm. Quartz tube around 0.4 milliliters