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近年来,随着毒品问题的日益泛滥,在一些个体食品摊点中出现了用罂粟壳作火锅调料的现象。为此我们对从陕西、贵州及河南三个省收集来的罂粟果实中的几个主要部分罂粟壳、罂粟籽及附带的罂粟杆中的阿片成分进行了分析;并建立了一个比较合理的分析方法。首先用酸浸泡粉碎后的样品,取出酸液后调成碱性并用含内标的有机溶剂提取,提取溶剂挥干后用甲醇定溶,用GC/FID进行分析并用内标法计算含量。该方法简变可靠,对吗啡、可待因、蒂巴因及罂粟碱的相对偏差分别为8.2%、3.0%、1.8%和1.4%,因而适用于作普查时对大量样品
In recent years, with the increasing proliferation of drugs, poppy shell has been used as a hotpot seasoning in some individual food stalls. To this end, we analyzed the opium components in poppyseed, poppyseeds and incidental poppy straw, which are the main parts of the poppy fruit collected from Shaanxi, Guizhou and Henan provinces. We also established a more reasonable analysis method. First acid soaked crushed samples, remove the acid and transferred into alkaline and containing internal standard organic solvent extraction, the solvent was evaporated to dryness with methanol, using GC / FID for analysis and content by internal standard method. The method is simple and reliable, with relative deviations of 8.2%, 3.0%, 1.8% and 1.4% for morphine, codeine, tetbarbine and papaverine, respectively. Therefore, this method is suitable for mass spectrometry