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Three complexes [AMP][Ni(mnt)2]·CH3CN(1, AMP = 1-(9-anthrylmethyl)pyridinium), [DPI]2[Ni(mnt)2]I(2, DPI = diphenyliodonium) and [DD][Ni(mnt)2]2·2H2O(3, DD = dimethylenediamine) have been prepared and characterized by elemental analyses and IR sp