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合成了含硫席夫碱试剂1-苯基-3-甲基-4-(α-呋喃甲酰基)吡唑啉酮-5缩氨基硫脲(L)及其铜,银的配合物。元素分析及摩尔电导值表明新配合物的组成为[CuL2]·4H2O,[AgL]NO3·C2H5OH。通过红外光谱、紫外光谱、差热-热重对配合物进行表征。
Synthesis of sulfur-containing Schiff base reagent 1-phenyl-3-methyl-4- (α-furoyl) pyrazolone -5 thiosemicarbazone (L) and copper, silver complexes. Elemental analysis and molar conductivity showed that the new complex was composed of [CuL2] · 4H2O, [AgL] NO3 · C2H5OH. The complexes were characterized by FTIR, UV-Vis, DTA-TG.