论文部分内容阅读
The title complex [(C8H23N4)3+ (ClO4)3-]. H2O was crystallized intriclinic system, P1 space group with unite cell parameters: a= 8. 386(2), b= 10. 558(2), c=11. 865(3) A, a= 77. 75(2)’ β= 72. 65(2),γ= 74. 77(2)°, V= 957. 3(4)A3, Z= 2, Dc= 1. 706 g/cm3, M,=491. 66, F(000) = 512, μ(MoKa) =5. 49cm-1,=0. 71069 (graphite- monochromated), T = 296K. The title complex is composed ofone [C8H23N4]3+ cation, three ClO4 ions and one crystal water molecule. The final Rand Rw values are 0. 058 and 0. 068 respectively.
The title complex [(C8H23N4) 3 + (ClO4) 3-]. H2O was crystallized intriclinic system with P1 space group with unite cell parameters: a = 8. 386 (2), b = 10. 558 (2), c = A = 77. 75 (2) ’β = 72.65 (2), γ = 74.77 (2) °, V = 957. 3 (4) A3, Z = 2, Dc = 1. 706 g / cm3, M, = 491.66, F (000) = 512, MoKa = 5.49 cm-1, = 0. 71069 (graphite- monochromated), T = 296 K. The title complex is composed ofone [C8H23N4] 3+ cation, three ClO4 ions and one crystal water molecule. The final Rand Rw values are 0. 058 and 0. 068 respectively.