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在不添加任何模板剂的情况下,采用温和水热法,制备了一系列NaGd0.96-x(WO4)2∶0.04Tb3+,xEu3+(x=0,0.005,0.01,0.02,0.04,0.06,0.08,0.10,0.12,0.14,0.16,0.18)荧光粉。采用X射线粉末衍射仪(XRD)、扫描电子显微镜(SEM)以及荧光分光光度计分别对所得样品的物相结构、形貌粒度及发光性能进行分析表征。结果表明:所合成的样品为NaGd(WO4)2的纯相,属四方晶系白钨矿结构。其形貌为规整的四方盘形,尺寸均一、分散性良好。系列样品均